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Lipopolysaccharide


DATA No : CLS0422 INFORMANT : Yoshio Kumazawa

NAME : 2'N-3''(dodecanoyloxy)tetradecanoyl, 3'-O-3''(tetradecanoyloxy)tetradecanoyl b-(1a_right6) D-glucosaminyl 2N-3''hydroxytetradecanoyl,3-O-3''hydroxytetradecanoyl D-glucosamine 1,4'-bisphosphate

COMMON NAME:
SYMBOL:
FORMULA: C94H176O25N2P2 MOL.WT (average) : 1796.349


Download ChemDraw structure data
BIOLOGICAL ACTIVITY

PHYSICAL AND CHEMICAL PROPERTIES
MELTING POINT:

BOILING POINT:

REFRACTIVE INDEX:

OPTICAL ROTATION:

DENSITY:

SOLUBILITY:
SPECTRAL DATA
UV SPECTRA:

IR SPECTRA:

NMR SPECTRA:1H-1H shift correlation spectrum at 500 MHz of HPLC-purified hexamethyl hexaacyl Re-LPS
[Spectrum 0019]
Proton NMR spectrum of the HPLC-purified hexamethyl hexaacyl Re-LPS
[Spectrum 0021]
13C and 13C-DEPT spectra
[Spectrum 0022]

MASS SPECTRA:Partial PD mass spectrum of HPLC-purified hexamethyl hexaacyl Re-LPS
[Spectrum 0020]

OTHER SPECTRA:
CHROMATOGRAM DATA
Reverse-phase HPLC of hexamethyl Re-LPS
[Chromatogram 0004]
Gel permeation chromatography of hexamethyl Re-LPS
[Chromatogram 0005]
SOURCE
Escherichia coli D31m4(Ref. 0422)
CHEMICAL SYNTHESIS

METABOLISM

GENETIC INFORMATION

NOTE
Quantitation of the phosphorus content of the HPLC-purified methylated Re-LPS
[Table 0014]
REFERENCES
[0422]
AUTHOR:Qureshi, N., Takayama, K., Mascagni, P., Honovich, J., Wong, R., and Cotter, R. J.
TITLE:Complete structural determination of lipopolysaccharide obtained from deep rough mutant of Escherichia coli. Purification by high performance liquid chromatography and direct analysis by plasma desorption mass spectrometry PubMed ID:3136169
JOURNAL:J Biol Chem.
VOL:263 PAGE : 11971-11976 (1988)
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Last updated June 19, 2007. Copyright © 1989-2007 Japanese Conference on the Biochemistry of Lipids (JCBL). All rights reserved.