|
| COMMON NAME | : | Stigmasterol, Anti-stiffness factor / 3b-Hydroxy-24-ethyl-D5,22-cholestadiene |
| SYMBOL | : | |
| FORMULA | : | C29H48O1 MOL.WT (average) : 412.691 |
| BIOLOGICAL ACTIVITY |
| PHYSICAL AND CHEMICAL PROPERTIES |
| MELTING POINT | : | 144.0-144.6 C (acetate), 170C (free) (Ref. 0170/0171/0172) |
| BOILING POINT | : | |
| REFRACTIVE INDEX | : | |
| OPTICAL ROTATION | : | [a]22/D = -51 (c = 2 in chloroform), [a]20/D = -55.6(acetate, c = 2 in chloroform) (Ref. 0171/0172) |
| DENSITY | : | |
| SOLUBILITY | : | Insol in water. Sol in organic solvents (Ref. 0172) |
| SPECTRAL DATA |
| UV SPECTRA | : | |
| IR SPECTRA | : | |
| NMR SPECTRA | : | |
| MASS SPECTRA | : | TMS : 484(22%), 394(35%), 255(63%), 145(32%), 133(38%), 129(100%) (Ref. 0148) |
| OTHER SPECTRA | : | |
| CHROMATOGRAM DATA |
| SOURCE |
| CHEMICAL SYNTHESIS |
| METABOLISM |
| GENETIC INFORMATION |
| NOTE |
| REFERENCES |
| AUTHOR | : | Steel, G., and Henderson, W. |
| TITLE | : | Rapid method for detection and characterization of steroids PubMed ID:4658153 |
| JOURNAL | : | Anal Chem. |
| VOL | : | 44 PAGE : 1302-1304 (1972) |
| AUTHOR | : | Deuel,Jr.,H.J.(1951) Waxes, Higher Alcohols including Sterols, Triterpenes, Glyceryl Ethers, Colored Fats, and Hydrocarbons in the Lipids Their Chemistry and Biochemistry I (Deuel,Jr.,H.J., eds) pp305-404, Interscience Publishers, New York |
| TITLE | : | |
| JOURNAL | : | |
| VOL | : | PAGE : - () |
| AUTHOR | : | Sandqvist,H., and Gorton,J. |
| TITLE | : | Stigmasterol and Its Empirical Formula. |
| JOURNAL | : | Ber. |
| VOL | : | 63 PAGE : 1935 -1938 (1930) |
| AUTHOR | : | Monographs in the Merck Index an encyclopedia of chemicals, drugs, and biologicals (Budavari,S., O'Neil,M.J., Smith,A., and Heckelman,P.E.,eds. 1989), pp1388-1388, MERCK & CO., Inc. Rahway, N.J. |
| TITLE | : | |
| JOURNAL | : | |
| VOL | : | PAGE : - () |
| AUTHOR | : | Windaus,A., and Hauth,A. |
| TITLE | : | Ueber Stigmasterin, Ein Neues Phytosterin aus Calabar-Bohnen. |
| JOURNAL | : | Ber. |
| VOL | : | 39 PAGE : 4378 -4384 (1906) |
| AUTHOR | : | Otto,A.C., and Ball,C.D. |
| TITLE | : | The Isolation of Stigmasterol and b-Sitosterol from the Common Bean, Phaseolus Vulgaris. |
| JOURNAL | : | J.Am.Chem.Soc. |
| VOL | : | 66 PAGE : 489 -491 (1944) |
| AUTHOR | : | Byerrum,R.U., and Ball,C.D. |
| TITLE | : | Stigmasterol. |
| JOURNAL | : | Biochem.Prepns. |
| VOL | : | 7 PAGE : 86 -88 (1959) |
| AUTHOR | : | Thornton,M.H., Kraybill,H.R., and Mitchell,Jr.,J.H. |
| TITLE | : | Sterol Glucosides from Expressed Soybean Oil. |
| JOURNAL | : | J.Am.Chem.Soc. |
| VOL | : | 62 PAGE : 2006 -2008 (1940) |
| AUTHOR | : | Rosenkrantz,H., Milhorat,A.T., Farber,M., and Milman,A.E. |
| TITLE | : | Purification and Identification of the Antistiffeness Factor. |
| JOURNAL | : | Proc.Soc.Exptl.Biol.Med. |
| VOL | : | 76 PAGE : 408 -410 (1951) |
| AUTHOR | : | Colin,H., Guiochon,G., and Siouffi,A. |
| TITLE | : | Comparison of Various Systems for the Separation of Free Sterols by High Performance Liquid Chromatography. |
| JOURNAL | : | Anal.Chem. |
| VOL | : | 51 PAGE : 1661 -1666 (1979) |